HKDSE · Thinka-original Practice Paper

2021 HKDSE Chemistry Practice Paper | DSE Mock

Thinka 2021 DSE-Style Mock — Chemistry

160 marks210 mins2021
An original Thinka practice paper modelled on the structure and difficulty of that year's HKDSE paper. Not affiliated with or reproduced from the HKEAA.

Paper 1 Section A

Answer ALL questions. All questions carry equal marks. Choose the best answer for each question.
36 Question · 36 marks
Question 1 · MC
1 marks
Which of the following processes does NOT involve oxidation or reduction?
  1. A.Reaction of chlorine with cold sodium hydroxide solution.
  2. B.Action of concentrated sulfuric acid on sodium chloride.
  3. C.Thermal decomposition of copper(II) nitrate.
  4. D.Action of hot concentrated nitric acid on carbon.
Question 2 · MC
1 marks
Given the following standard enthalpy changes of combustion (\(\Delta H_c^\theta\)): Carbon, \(\text{C(s, graphite)} = -393.5\text{ kJ mol}^{-1}\); Hydrogen, \(\text{H}_2\text{(g)} = -285.8\text{ kJ mol}^{-1}\); Ethanol, \(\text{C}_2\text{H}_5\text{OH(l)} = -1367.3\text{ kJ mol}^{-1}\). What is the standard enthalpy change of formation of ethanol (\(\text{C}_2\text{H}_5\text{OH(l)}\))?
  1. A.\(-277.1\text{ kJ mol}^{-1}\)
  2. B.\(+277.1\text{ kJ mol}^{-1}\)
  3. C.\(-688.0\text{ kJ mol}^{-1}\)
  4. D.\(+688.0\text{ kJ mol}^{-1}\)
Question 3 · MC
1 marks
Which of the following combinations of reagents and conditions is most suitable for converting propan-1-ol to propan-2-ol?
  1. A.Step 1: Heat with excess concentrated \(\text{H}_2\text{SO}_4\) at \(170\ ^\circ\text{C}\); Step 2: Heat with \(\text{H}_2\text{O}\) in the presence of \(\text{H}^+\)
  2. B.Step 1: Reflux with acidified \(\text{K}_2\text{Cr}_2\text{O}_7\text{(aq)}\); Step 2: React with \(\text{NaBH}_4\)
  3. C.Step 1: Reflux with concentrated \(\text{HCl}\text{(aq)}\) in the presence of anhydrous \(\text{ZnCl}_2\); Step 2: Heat with \(\text{NaOH}\text{(aq)}\)
  4. D.Step 1: React with \(\text{PBr}_3\); Step 2: Heat with \(\text{KOH(aq)}\)
Question 4 · MC
1 marks
Three metals, \(X\), \(Y\), and \(Z\), have the following properties: (1) Oxide of \(X\) can be reduced by heating with carbon, but oxide of \(Y\) cannot. (2) When a piece of metal \(X\) is placed in an aqueous solution of nitrate of \(Z\), a grey deposit is formed on the surface of \(X\). (3) Metal \(Y\) reacts with cold water to liberate hydrogen gas, while metal \(X\) does not. Which of the following arrangements shows the order of reactivity of these metals (from the most reactive to the least reactive)?
  1. A.\(Y > X > Z\)
  2. B.\(Y > Z > X\)
  3. C.\(X > Y > Z\)
  4. D.\(Z > Y > X\)
Question 5 · MC
1 marks
A reaction has a rate constant \(k_1 = 2.0 \times 10^{-3}\text{ s}^{-1}\) at \(300\text{ K}\), and \(k_2 = 8.0 \times 10^{-3}\text{ s}^{-1}\) at \(320\text{ K}\). What is the activation energy (\(E_a\)) of this reaction? (Given: Gas constant \(R = 8.31\text{ J mol}^{-1}\text{ K}^{-1}\))
  1. A.\(55.3\text{ kJ mol}^{-1}\)
  2. B.\(110.6\text{ kJ mol}^{-1}\)
  3. C.\(23.0\text{ kJ mol}^{-1}\)
  4. D.\(5.53\text{ kJ mol}^{-1}\)
Question 6 · MC
1 marks
Consider an alkaline hydrogen-oxygen fuel cell. Which of the following statements is/are correct? (1) The reaction at the anode is \(\text{O}_2\text{(g)} + 2\text{H}_2\text{O(l)} + 4e^- \rightarrow 4\text{OH}^-\text{(aq)}\). (2) Potassium hydroxide solution is commonly used as the electrolyte. (3) The overall cell reaction produces water as the only product.
  1. A.(1) only
  2. B.(2) only
  3. C.(1) and (3) only
  4. D.(2) and (3) only
Question 7 · MC
1 marks
A \(1.50\text{ g}\) sample of impure limestone (mainly containing \(\text{CaCO}_3\)) was reacted with \(50.0\text{ cm}^3\) of \(0.500\text{ M HCl(aq)}\). After the reaction was complete, the excess acid required \(15.0\text{ cm}^3\) of \(0.200\text{ M NaOH(aq)}\) for complete neutralization. What is the percentage by mass of \(\text{CaCO}_3\) in the sample? (Molar mass of \(\text{CaCO}_3 = 100.1\text{ g mol}^{-1}\))
  1. A.73.4%
  2. B.83.4%
  3. C.36.7%
  4. D.93.4%
Question 8 · MC
1 marks
Which of the following pairs of compounds cannot be distinguished by identifying characteristic functional group absorptions in infrared (IR) spectroscopy alone?
  1. A.Ethanol and ethanoic acid
  2. B.Propan-1-ol and propanal
  3. C.Ethanoic acid and ethyl ethanoate
  4. D.Methyl propanoate and ethyl ethanoate
Question 9 · MC
1 marks
Which of the following groups of species all have a trigonal planar shape?
  1. A.\(\text{BF}_3\), \(\text{CO}_3^{2-}\), \(\text{NO}_3^-\)
  2. B.\(\text{NH}_3\), \(\text{PCl}_3\), \(\text{H}_3\text{O}^+\)
  3. C.\(\text{CH}_4\), \(\text{SiF}_4\), \(\text{NH}_4^+\)
  4. D.\(\text{O}_3\), \(\text{SO}_2\), \(\text{NO}_2^-\)
Question 10 · MC
1 marks
Maleic anhydride (\(\text{C}_4\text{H}_2\text{O}_3\)) can be produced by the catalytic oxidation of butene as shown in the equation below: \(\text{C}_4\text{H}_8 + 3\text{O}_2 \rightarrow \text{C}_4\text{H}_2\text{O}_3 + 3\text{H}_2\text{O}\). What is the atom economy of this reaction for the production of maleic anhydride? (Relative atomic masses: \(\text{H} = 1.0\), \(\text{C} = 12.0\), \(\text{O} = 16.0\))
  1. A.64.5%
  2. B.44.1%
  3. C.84.5%
  4. D.35.5%
Question 11 · MC
1 marks
Consider the following thermochemical equations:
1) \( \text{C(graphite)} + \text{O}_2\text{(g)} \rightarrow \text{CO}_2\text{(g)} \quad \Delta H_1 = -393.5 \text{ kJ mol}^{-1} \)
2) \( \text{H}_2\text{(g)} + \frac{1}{2}\text{O}_2\text{(g)} \rightarrow \text{H}_2\text{O(l)} \quad \Delta H_2 = -285.8 \text{ kJ mol}^{-1} \)
3) \( 2\text{C(graphite)} + 3\text{H}_2\text{(g)} + \frac{1}{2}\text{O}_2\text{(g)} \rightarrow \text{C}_2\text{H}_5\text{OH(l)} \quad \Delta H_3 = -277.6 \text{ kJ mol}^{-1} \)

What is the standard enthalpy change of combustion of liquid ethanol (\( \text{C}_2\text{H}_5\text{OH(l)} \))?
  1. A.\( -1366.8 \text{ kJ mol}^{-1} \)
  2. B.\( -956.8 \text{ kJ mol}^{-1} \)
  3. C.\( -401.7 \text{ kJ mol}^{-1} \)
  4. D.\( -1921.8 \text{ kJ mol}^{-1} \)
Question 12 · MC
1 marks
Which of the following processes involves an oxidation in which the oxidation number of sulfur increases by exactly 4?
  1. A.Burning sulfur in excess oxygen to form sulfur dioxide.
  2. B.Reaction of hydrogen sulfide with sulfur dioxide to form sulfur.
  3. C.Reaction of sulfur dioxide with acidified potassium dichromate(VI) solution.
  4. D.Reaction of copper with concentrated sulfuric acid to produce sulfur dioxide.
Question 13 · MC
1 marks
What is the systematic IUPAC name of the compound below?
\( \text{CH}_3\text{CH(CH}_3\text{)C(CH}_3\text{)=CHCH}_3 \)
  1. A.2,3-dimethylpent-3-ene
  2. B.3,4-dimethylpent-2-ene
  3. C.2,3-dimethylpent-2-ene
  4. D.1,2,3-trimethylbut-2-ene
Question 14 · MC
1 marks
An organic compound \( X \) has the molecular formula \( \text{C}_4\text{H}_8\text{O} \). It does not react with acidified potassium dichromate(VI) solution upon warming, nor does it react with sodium metal. Which of the following is the correct structure of \( X \)?
  1. A.\( \text{CH}_3\text{CH}_2\text{CH}_2\text{CHO} \)
  2. B.\( \text{CH}_3\text{CH(OH)CH=CH}_2 \)
  3. C.\( \text{CH}_3\text{COCH}_2\text{CH}_3 \)
  4. D.\( \text{CH}_2\text{=CHCH}_2\text{CH}_2\text{OH} \)
Question 15 · MC
1 marks
The rate constant \( k \) of a certain reaction was measured at different temperatures. A plot of \( \ln k \) against \( \frac{1}{T} \) (where \( T \) is temperature in Kelvin) yielded a straight line with a slope of \( -1.20 \times 10^4 \text{ K} \). What is the activation energy (\( E_a \)) of this reaction?
(Given: Gas constant \( R = 8.31 \text{ J mol}^{-1}\text{ K}^{-1} \))
  1. A.\( 1.44 \text{ kJ mol}^{-1} \)
  2. B.\( 14.4 \text{ kJ mol}^{-1} \)
  3. C.\( 99.7 \text{ kJ mol}^{-1} \)
  4. D.\( 997 \text{ kJ mol}^{-1} \)
Question 16 · MC
1 marks
Maleic anhydride (\( \text{C}_4\text{H}_2\text{O}_3 \)) can be synthesized via two different routes:
Route 1: \( 2\text{C}_6\text{H}_6 + 9\text{O}_2 \rightarrow 2\text{C}_4\text{H}_2\text{O}_3 + 4\text{CO}_2 + 4\text{H}_2\text{O} \)
Route 2: \( \text{C}_4\text{H}_8 + 3\text{O}_2 \rightarrow \text{C}_4\text{H}_2\text{O}_3 + 3\text{H}_2\text{O} \)

Which route is greener according to the principle of atom economy?
(Relative atomic masses: \( \text{H} = 1.0 \), \( \text{C} = 12.0 \), \( \text{O} = 16.0 \))
  1. A.Route 1 is greener because its atom economy is 64.5%, compared to 44.1% for Route 2.
  2. B.Route 2 is greener because its atom economy is 64.5%, compared to 44.1% for Route 1.
  3. C.Route 1 is greener because its atom economy is 55.9%, compared to 35.5% for Route 2.
  4. D.Route 2 is greener because its atom economy is 82.1%, compared to 17.9% for Route 1.
Question 17 · MC
1 marks
A \( 25.00 \text{ cm}^3 \) sample of commercial bleach containing sodium hypochlorite (\( \text{NaOCl} \)) was diluted to \( 250.0 \text{ cm}^3 \). A \( 25.00 \text{ cm}^3 \) portion of this diluted solution was acidified and reacted with excess KI(aq). The liberated iodine required \( 22.40 \text{ cm}^3 \) of \( 0.100 \text{ mol dm}^{-3} \) \( \text{Na}_2\text{S}_2\text{O}_3\text{(aq)} \) for complete titration.

What is the concentration of \( \text{NaOCl} \) in the original commercial bleach?
(Equations:
\( \text{OCl}^- + 2\text{I}^- + 2\text{H}^+ \rightarrow \text{Cl}^- + \text{I}_2 + \text{H}_2\text{O} \)
\( \text{I}_2 + 2\text{S}_2\text{O}_3^{2-} \rightarrow 2\text{I}^- + \text{S}_4\text{O}_6^{2-} \))
  1. A.\( 0.0448 \text{ mol dm}^{-3} \)
  2. B.\( 0.224 \text{ mol dm}^{-3} \)
  3. C.\( 0.448 \text{ mol dm}^{-3} \)
  4. D.\( 0.896 \text{ mol dm}^{-3} \)
Question 18 · MC
1 marks
An organic compound \( Y \) has a molecular formula \( \text{C}_3\text{H}_6\text{O}_2 \). Its infrared (IR) spectrum shows a strong broad absorption band around \( 3000 \text{ cm}^{-1} \) and a strong sharp absorption band around \( 1715 \text{ cm}^{-1} \). Which of the following statements about the mass spectrum of \( Y \) is correct?
  1. A.The molecular ion peak occurs at \( m/z = 60 \).
  2. B.It shows a prominent peak at \( m/z = 45 \), corresponding to the species \( [\text{COOH}]^+ \).
  3. C.It shows a prominent peak at \( m/z = 43 \), corresponding to the species \( [\text{C}_3\text{H}_7]^+ \).
  4. D.There is a prominent peak at \( m/z = 15 \) due to the loss of a water molecule.
Question 19 · MC
1 marks
Which of the following mixtures, when heated strongly, will undergo a displacement reaction?
  1. A.\( \text{MgO} \) and \( \text{Fe} \)
  2. B.\( \text{Al}_2\text{O}_3 \) and \( \text{Cu} \)
  3. C.\( \text{Fe}_2\text{O}_3 \) and \( \text{Al} \)
  4. D.\( \text{ZnO} \) and \( \text{Pb} \)
Question 20 · MC
1 marks
Which of the following molecules / ions has the same shape as the hydronium ion (\( \text{H}_3\text{O}^+ \))?
  1. A.\( \text{BF}_3 \)
  2. B.\( \text{PCl}_3 \)
  3. C.\( \text{CO}_3^{2-} \)
  4. D.\( \text{ClF}_3 \)
Question 21 · MC
1 marks
Consider the following standard enthalpy changes of combustion (\(\Delta H_c^\theta\)) at \(298\text{ K}\): \(\text{C(graphite)} = -393.5\text{ kJ mol}^{-1}\), \(\text{H}_2\text{(g)} = -285.8\text{ kJ mol}^{-1}\), \(\text{C}_3\text{H}_8\text{(g)} = -2220.0\text{ kJ mol}^{-1}\). What is the standard enthalpy change of formation of propane (\(\text{C}_3\text{H}_8\text{(g)}\)) at \(298\text{ K}\)?
  1. A.-103.7 kJ mol^{-1}
  2. B.-1540.7 kJ mol^{-1}
  3. C.+103.7 kJ mol^{-1}
  4. D.+1540.7 kJ mol^{-1}
Question 22 · MC
1 marks
A chemical cell is set up by connecting a zinc-zinc(II) ion half-cell and a copper-copper(II) ion half-cell using a salt bridge. If the zinc electrode and its solution are replaced by a nickel electrode and a nickel(II) ion solution under the same conditions, which of the following statements is/are correct? (Given standard reduction potentials: \(E^\theta(\text{Zn}^{2+}/\text{Zn}) = -0.76\text{ V}\); \(E^\theta(\text{Ni}^{2+}/\text{Ni}) = -0.25\text{ V}\); \(E^\theta(\text{Cu}^{2+}/\text{Cu}) = +0.34\text{ V}\)) (1) The cell voltage decreases. (2) Electrons still flow from the other electrode to the copper electrode through the external circuit. (3) The mass of the nickel electrode increases.
  1. A.(1) only
  2. B.(1) and (2) only
  3. C.(2) and (3) only
  4. D.(1), (2) and (3)
Question 23 · MC
1 marks
What is the IUPAC name of the compound with the following structure? \(\text{ClCH}_2\text{CH}=\text{CHCH(CH}_3)_2\)
  1. A.5-chloro-2-methylpent-3-ene
  2. B.1-chloro-4-methylpent-2-ene
  3. C.1-chloro-4,4-dimethylbut-2-ene
  4. D.4-isopropyl-1-chlorobut-2-ene
Question 24 · MC
1 marks
Consider the following reaction route: Compound X \(\xrightarrow{\text{acidified }\text{K}_2\text{Cr}_2\text{O}_7\text{(aq), heat under reflux}}\). Compound Y \(\xrightarrow{\text{CH}_3\text{CH}_2\text{OH, conc. }\text{H}_2\text{SO}_4\text{, heat}}\). Compound Z. If Compound Z has the molecular formula \(\text{C}_5\text{H}_{10}\text{O}_2\), what is the IUPAC name of Compound X?
  1. A.propan-1-ol
  2. B.propan-2-ol
  3. C.propanoic acid
  4. D.ethyl propanoate
Question 25 · MC
1 marks
A \(2.50\text{ g}\) sample of an eggshell was treated with \(50.0\text{ cm}^3\) of \(0.500\text{ M }\text{HCl(aq)}\). After the reaction was complete, the remaining solution required \(16.8\text{ cm}^3\) of \(0.250\text{ M }\text{NaOH(aq)}\) for complete neutralization. What is the percentage by mass of calcium carbonate (\(\text{CaCO}_3\)) in the eggshell? (Relative atomic masses: \(C = 12.0\), \(O = 16.0\), \(Ca = 40.1\))
  1. A.20.8%
  2. B.41.6%
  3. C.83.3%
  4. D.91.6%
Question 26 · MC
1 marks
For a particular chemical reaction, a plot of \(\ln k\) against \(\frac{1}{T}\) gives a straight line with a slope of \(-1.20 \times 10^4\text{ K}\), where \(k\) is the rate constant and \(T\) is the temperature in Kelvin. What is the activation energy of this reaction? (Given: gas constant \(R = 8.314\text{ J mol}^{-1}\text{ K}^{-1}\))
  1. A.99.8 kJ mol^{-1}
  2. B.1.44 kJ mol^{-1}
  3. C.12.0 kJ mol^{-1}
  4. D.99.8 J mol^{-1}
Question 27 · MC
1 marks
Acetanilide (\(\text{C}_8\text{H}_9\text{NO}\)) is prepared by reacting aniline (\(\text{C}_6\text{H}_5\text{NH}_2\)) with acetic anhydride (\((\text{CH}_3\text{CO})_2\text{O}\)) according to the following equation: \(\text{C}_6\text{H}_5\text{NH}_2 + (\text{CH}_3\text{CO})_2\text{O} \rightarrow \text{C}_6\text{H}_5\text{NHCOCH}_3 + \text{CH}_3\text{COOH}\). What is the atom economy of this reaction for the synthesis of acetanilide? (Relative atomic masses: \(H = 1.0\), \(C = 12.0\), \(N = 14.0\), \(O = 16.0\))
  1. A.30.8%
  2. B.44.4%
  3. C.69.2%
  4. D.100%
Question 28 · MC
1 marks
An organic compound X shows a strong and broad absorption band in the range \(3230 - 3670\text{ cm}^{-1}\) in its infrared spectrum. Compound X does not cause any color change when heated with acidified \(\text{K}_2\text{Cr}_2\text{O}_7\text{(aq)}\). Which of the following is most likely Compound X?
  1. A.propan-1-ol
  2. B.propan-2-ol
  3. C.2-methylpropan-2-ol
  4. D.propanoic acid
Question 29 · MC
1 marks
Consider the following experimental observations on three metals, P, Q, and R: (1) Metal P reacts vigorously with cold water to produce a gas. (2) The oxide of Q can be reduced by heating with carbon, but the oxide of P cannot. (3) When metal Q is added to an aqueous solution containing ions of R, a deposit of metal R is formed on the surface of Q. Which of the following is the correct order of reactivity of the metals in decreasing order?
  1. A.P > Q > R
  2. B.P > R > Q
  3. C.Q > P > R
  4. D.R > Q > P
Question 30 · MC
1 marks
Which of the following pairs of chemical species has the same molecular / ionic shape?
  1. A.BF3 and NH3
  2. B.CH4 and NH4+
  3. C.H2O and CO2
  4. D.PCl3 and BF3
Question 31 · MC
1 marks
Consider the following standard enthalpy changes:
\( \text{C(graphite)} + \text{O}_2\text{(g)} \rightarrow \text{CO}_2\text{(g)} \quad \Delta H^\theta = -393.5 \text{ kJ mol}^{-1} \)
\( 2\text{H}_2\text{(g)} + \text{O}_2\text{(g)} \rightarrow 2\text{H}_2\text{O(l)} \quad \Delta H^\theta = -571.6 \text{ kJ mol}^{-1} \)
\( 2\text{C}_2\text{H}_2\text{(g)} + 5\text{O}_2\text{(g)} \rightarrow 4\text{CO}_2\text{(g)} + 2\text{H}_2\text{O(l)} \quad \Delta H^\theta = -2598.8 \text{ kJ mol}^{-1} \)

What is the standard enthalpy change of formation of ethyne (\(\text{C}_2\text{H}_2\text{(g)}\))?
  1. A.-226.6 kJ mol^-1
  2. B.+113.3 kJ mol^-1
  3. C.+226.6 kJ mol^-1
  4. D.+453.2 kJ mol^-1
Question 32 · MC
1 marks
In which of the following species does vanadium have an oxidation number of +4?
(1) \(\text{VO}^{2+}\)
(2) \(\text{VO}_2\)
(3) \(\text{VCl}_4\)
  1. A.(1) and (2) only
  2. B.(1) and (3) only
  3. C.(2) and (3) only
  4. D.(1), (2) and (3)
Question 33 · MC
1 marks
An organic compound \(X\) has the molecular formula \(\text{C}_4\text{H}_8\text{O}_2\). It does not react with sodium metal to give hydrogen gas, nor does it react with sodium hydrogencarbonate solution. To which of the following homologous series could \(X\) belong?
  1. A.Carboxylic acids
  2. B.Esters
  3. C.Diols
  4. D.Alcohols
Question 34 · MC
1 marks
A mixture of gas \(X\) and gas \(Y\) reacts to form gas \(Z\). Which of the following changes would increase BOTH the rate of the reaction and the fraction of reactant molecules having energy equal to or greater than the activation energy?
(1) Increasing the temperature of the reaction mixture
(2) Adding a suitable catalyst
(3) Increasing the pressure of the system by reducing the volume of the container
  1. A.(1) only
  2. B.(1) and (2) only
  3. C.(2) and (3) only
  4. D.(1), (2) and (3)
Question 35 · MC
1 marks
How many acyclic structural isomers (excluding stereoisomers) exist for the compound with the molecular formula \(\text{C}_3\text{H}_5\text{Cl}_3\)?
  1. A.4
  2. B.5
  3. C.6
  4. D.7
Question 36 · MC
1 marks
In a standardisation experiment, a student transfers \(25.00 \text{ cm}^3\) of a standard sodium carbonate solution into a conical flask using a pipette, and titrates it against a hydrochloric acid solution of unknown concentration delivered from a burette.

Which of the following experimental errors would result in an OVERESTIMATION of the calculated concentration of the hydrochloric acid solution?
  1. A.Rinsing the pipette with distilled water only before transferring the sodium carbonate solution.
  2. B.Rinsing the conical flask with the sodium carbonate solution before the titration.
  3. C.Rinsing the burette with distilled water only before filling it with the hydrochloric acid solution.
  4. D.Leaving an air bubble in the tip of the burette which is dislodged during the titration.

Paper 1 Section B

Answer ALL questions in both Part I and Part II. Write your answers in the spaces provided.
13 Question · 78 marks
Question 1 · conventional
6 marks
An electrolysis experiment is set up to purify an impure sample of copper containing small amounts of zinc and silver as impurities. The electrolyte used is aqueous copper(II) sulfate. (a) State which electrode (anode or cathode) should be made of the impure copper sample, and explain your answer in terms of oxidation and reduction. (2 marks) (b) Describe what happens to the zinc and silver impurities during the electrolysis process. (2 marks) (c) Write the ionic half-equation for the reaction occurring at the cathode, and state the visible change at this electrode. (2 marks)
Question 2 · conventional
6 marks
A monomer X has the structure CH2=C(CH3)COOCH2CH3. (a) Give the systematic IUPAC name for monomer X. (1 mark) (b) Draw the repeating unit of the addition polymer formed from X. (1 mark) (c) Explain why this polymer is a thermoplastic rather than a thermosetting plastic. (2 marks) (d) Suggest one environmental concern associated with the disposal of this polymer by incineration. (2 marks)
Question 3 · conventional
6 marks
Titanium is extracted from its ore rutile (TiO2) via a multi-step process involving the reduction of titanium(IV) chloride (TiCl4) with magnesium at high temperatures. (a) Explain why titanium cannot be directly extracted from TiO2 by heating with carbon. (2 marks) (b) Write a chemical equation for the reduction of TiCl4 by magnesium. (1 mark) (c) Suggest why this extraction process is conducted under an inert atmosphere of argon gas. (1 mark) (d) State one advantage and one disadvantage of recycling titanium metal rather than extracting it from its ore. (2 marks)
Question 4 · conventional
6 marks
An experiment was conducted to determine the standard enthalpy change of formation of liquid propan-2-ol, CH3CH(OH)CH3(l). The standard enthalpy changes of combustion (\Delta H_c^\theta) are given: \Delta H_c^\theta[C(s, graphite)] = -394 kJ mol-1, \Delta H_c^\theta[H2(g)] = -286 kJ mol-1, \Delta H_c^\theta[CH3CH(OH)CH3(l)] = -2006 kJ mol-1. (a) Write the thermochemical equation for the standard enthalpy change of formation of propan-2-ol. (2 marks) (b) Construct a Hess's Law cycle to calculate the standard enthalpy change of formation (\Delta H_f^\theta) of propan-2-ol. (4 marks)
Question 5 · conventional
6 marks
Ethyl ethanoate is prepared in a laboratory by reacting ethanol with ethanoic acid. (a) Name the catalyst used in this reaction and state one other function of this substance in the reaction mixture. (2 marks) (b) Briefly explain why the reaction mixture is heated under reflux rather than in an open beaker. (2 marks) (c) After heating, sodium carbonate solution is added to the mixture. State the purpose of adding sodium carbonate and the observation that indicates its reaction is complete. (2 marks)
Question 6 · conventional
6 marks
The rate constant k of a first-order decomposition reaction was measured at two different temperatures: At T1 = 300 K, k1 = 2.4 * 10^-3 s-1. At T2 = 340 K, k2 = 6.8 * 10^-2 s-1. (Given: Gas constant R = 8.31 J K-1 mol-1; Arrhenius equation can be written as ln(k2/k1) = -Ea/R * (1/T2 - 1/T1)). (a) Calculate the activation energy, Ea, for this reaction in kJ mol-1. (4 marks) (b) Explain, using collision theory, how a catalyst increases the rate of this reaction. (2 marks)
Question 7 · conventional
6 marks
Consider the following two chemical routes, Route A and Route B, for producing a desired product P (molar mass = 120 g mol-1). Route A (Single-step): X + Y -> P + Z (molar mass of X = 80 g mol-1, Y = 90 g mol-1, and Z = 50 g mol-1). Route B (Two-step catalytic): Step 1: A + B -> C (100% yield); Step 2: C + D -> P (90% yield, no by-products) (molar mass of A = 50 g mol-1, B = 70 g mol-1, D = 10 g mol-1, and C = 120 g mol-1). (a) Calculate the atom economy of Route A. (2 marks) (b) Calculate the atom economy of Route B. (2 marks) (c) Based on green chemistry principles, suggest two reasons why Route B might be preferred over Route A, despite involving more steps. (2 marks)
Question 8 · conventional
6 marks
A student determined the calcium carbonate content of an eggshell. A 2.00 g sample of clean, dry eggshell was treated with 50.0 cm3 of 1.00 mol dm-3 hydrochloric acid, HCl(aq) (an excess). The mixture was heated to complete the reaction and filtered. The filtrate was made up to 250.0 cm3. A 25.0 cm3 portion of this solution required 14.10 cm3 of 0.100 mol dm-3 sodium hydroxide, NaOH(aq), for complete neutralisation. (a) Write the chemical equation for the reaction between calcium carbonate and hydrochloric acid. (1 mark) (b) Calculate the number of moles of HCl that reacted with the calcium carbonate in the eggshell sample. (4 marks) (c) Calculate the percentage by mass of calcium carbonate in the eggshell. (1 mark) (Molar mass of CaCO3 = 100.1 g mol-1)
Question 9 · conventional
6 marks
An unknown organic compound W has the molecular formula C3H6O. (a) Draw the structures of all possible structural isomers of W that are carbonyl compounds (aldehydes or ketones). (2 marks) (b) In the Infrared (IR) spectrum of W, a strong, sharp absorption peak is observed near 1715 cm-1, but there is no absorption peak in the region of 2700 - 2830 cm-1. Identify the functional group present in W, and deduce whether W is an aldehyde or a ketone. (2 marks) (c) Describe how you could use a chemical test to distinguish between the possible isomers in (a) and state the observations. (2 marks)
Question 10 · conventional
6 marks
Carbonyl chloride (COCl2) decomposes according to the following reversible equation: COCl2(g) <=> CO(g) + Cl2(g) (\Delta H > 0). In an experiment, 1.00 mol of COCl2(g) is introduced into a closed 2.00 dm3 vessel at 600 K. At equilibrium, the concentration of CO(g) is found to be 0.15 mol dm-3. (a) Write the expression for the equilibrium constant, Kc, for this reaction. (1 mark) (b) Calculate the equilibrium concentrations of COCl2(g) and Cl2(g), and hence determine the value of Kc at 600 K (with units). (3 marks) (c) Predict and explain the effect of increasing the temperature on the equilibrium yield of CO(g). (2 marks)
Question 11 · Structured
6 marks
An alkaline hydrogen-oxygen fuel cell is used in space shuttles to provide electricity and drinking water.
(a) Write the half-equation for the reaction occurring at the anode (negative electrode) of this cell. (1 mark)
(b) Write the half-equation for the reaction occurring at the cathode (positive electrode) of this cell. (1 mark)
(c) State one advantage of using fuel cells over conventional zinc-carbon dry cells. (1 mark)
(d) Under a certain operating condition, the fuel cell delivers a constant current of \(2.0\text{ A}\) for \(9650\text{ s}\). Calculate the mass of water produced during this period.
(Faraday constant, \(F = 96500\text{ C mol}^{-1}\); molar mass of \(\text{H}_2\text{O} = 18.0\text{ g mol}^{-1}\)) (3 marks)
Question 12 · Structured
6 marks
The standard enthalpy changes of combustion (\(\Delta H_c^\ominus\)) of carbon (graphite), hydrogen gas, and propene gas (\(\text{C}_3\text{H}_6\)) at \(298\text{ K}\) are given below:
- \(\text{C}\text{(graphite, } s) + \text{O}_2(g) \rightarrow \text{CO}_2(g) \quad \Delta H_c^\ominus = -394\text{ kJ mol}^{-1}\)
- \(\text{H}_2(g) + \frac{1}{2}\text{O}_2(g) \rightarrow \text{H}_2\text{O}(l) \quad \Delta H_c^\ominus = -286\text{ kJ mol}^{-1}\)
- \(\text{C}_3\text{H}_6(g) + \frac{9}{2}\text{O}_2(g) \rightarrow 3\text{CO}_2(g) + 3\text{H}_2\text{O}(l) \quad \Delta H_c^\ominus = -2058\text{ kJ mol}^{-1}\)

(a) Define the term "standard enthalpy change of combustion". (2 marks)
(b) Write a chemical equation for the formation of propene gas from its elements in their standard states. (1 mark)
(c) Calculate the standard enthalpy change of formation of propene gas. (3 marks)
Question 13 · Structured
6 marks
Consider the following reaction sequence to prepare ethyl propanoate from 1-chloropropane:
Reaction 1: \(\text{1-chloropropane} \xrightarrow{\text{reagent A}} \text{propan-1-ol}\)
Reaction 2: \(\text{propan-1-ol} \xrightarrow{\text{reagent B}} \text{propanoic acid}\)
Reaction 3: \(\text{propanoic acid} + \text{ethanol} \xrightarrow{\text{reagent C}} \text{ethyl propanoate}\)

(a) State the reagent and reaction conditions for Reaction 1. (2 marks)
(b) Identify reagent B and state the expected color change during Reaction 2. (2 marks)
(c) State the name of reagent C and its role in Reaction 3. (2 marks)

Paper 2 Section A (Industrial Chemistry)

Answer ALL parts of the question. Show your calculations where necessary.
1 Question · 20 marks
Question 1 · Structured
20 marks
Answer ALL parts of the question. Show your calculations where necessary.

(a) Carbon dioxide hydrogenation to methanol is a promising pathway for \(\text{CO}_2\) utilization. The rate constants (\(k\)) for this catalytic reaction were measured at two different temperatures:
At \(500\text{ K}\), \(k_1 = 2.5 \times 10^{-3}\text{ s}^{-1}\)
At \(550\text{ K}\), \(k_2 = 1.5 \times 10^{-2}\text{ s}^{-1}\)

(i) Calculate the activation energy (\(E_a\)) for this reaction in \(\text{kJ mol}^{-1}\).
(Given: Gas constant \(R = 8.31\text{ J K}^{-1}\text{ mol}^{-1}\)) (4 marks)

(ii) Sketch a Maxwell-Boltzmann distribution curve of molecular kinetic energies at \(500\text{ K}\) and \(550\text{ K}\). Explain how the change in temperature affects the rate of reaction. (3 marks)

(b) The equation for the synthesis of methanol from carbon dioxide is:

\(\text{CO}_2(\text{g}) + 3\text{H}_2(\text{g}) \rightleftharpoons \text{CH}_3\text{OH}(\text{g}) + \text{H}_2\text{O}(\text{g}) \quad \Delta H = -49.5\text{ kJ mol}^{-1}\)

(i) Predict and explain the effects of increasing the temperature and increasing the pressure on the equilibrium yield of methanol. (4 marks)

(ii) In industry, the reaction is typically carried out at a compromise temperature of \(250^\circ\text{C}\) and a pressure of \(50\text{ atm}\). Explain why these conditions are used by considering kinetic, thermodynamic, and economic/safety factors. (3 marks)

(c) Methanol can be synthesized via different industrial pathways:

Pathway 1: \(\text{CO}(\text{g}) + 2\text{H}_2(\text{g}) \rightarrow \text{CH}_3\text{OH}(\text{g})\)

Pathway 2: \(\text{CO}_2(\text{g}) + 3\text{H}_2(\text{g}) \rightarrow \text{CH}_3\text{OH}(\text{g}) + \text{H}_2\text{O}(\text{g})\)

(i) Calculate the atom economy of both Pathway 1 and Pathway 2 for the synthesis of methanol.
(Relative atomic masses: \(\text{H} = 1.0\), \(\text{C} = 12.0\), \(\text{O} = 16.0\)) (3 marks)

(ii) Even though Pathway 2 has a lower atom economy, explain why it is preferred in terms of green chemistry principles. (2 marks)

(iii) The copper-based catalyst used in this process is easily poisoned by trace amounts of sulfur compounds (such as \(\text{H}_2\text{S}\)) present in the reactant gas mixture.

(1) Explain, in terms of activation energy, how a catalyst increases the reaction rate. (1 mark)

(2) State how sulfur compounds "poison" the catalyst, and suggest one method to prevent this in the industrial process. (2 marks)

Paper 2 Section C (Analytical Chemistry)

Answer ALL parts of the question. Show your calculations where necessary.
1 Question · 20 marks
Question 1 · Structured
20 marks
An analytical chemist is investigating the purity of a solvent and analyzing an industrial wastewater effluent. This question consists of three parts.

**Part (a) (8 marks)**
An organic compound \(A\) is a common solvent used in cosmetics. It has the molecular formula \(C_4H_8O_2\).
(i) Describe a chemical test to distinguish whether \(A\) is a carboxylic acid or an ester. (2 marks)
(ii) The infrared (IR) spectrum of \(A\) shows a strong absorption band at \(1740\text{ cm}^{-1}\) but no broad absorption band in the region \(2500 - 3300\text{ cm}^{-1}\).
(1) What functional group is present in \(A\) based on this information? (1 mark)
(2) Explain why the absence of a broad band in the region \(2500 - 3300\text{ cm}^{-1}\) rules out certain isomers of \(C_4H_8O_2\). (1 mark)
(iii) The mass spectrum of \(A\) shows a base peak at \(m/z = 43\), and other prominent peaks at \(m/z = 88\) (molecular ion peak) and \(m/z = 61\).
(1) Suggest the structure of the species responsible for the peak at \(m/z = 43\). (1 mark)
(2) Deduce the structural formula of \(A\). Explain your reasoning. (3 marks)

**Part (b) (7 marks)**
A chemist determines the concentration of \(\text{Cr}_2\text{O}_7^{2-}(aq)\) ions in an industrial wastewater sample using colorimetry.
(i) Explain why \(\text{Cr}_2\text{O}_7^{2-}(aq)\) can be analyzed quantitatively using colorimetry. (1 mark)
(ii) Briefly explain how a colorimeter works and why a complementary filter is chosen for this analysis. (2 marks)
(iii) The chemist prepared a series of standard solutions of \(\text{Cr}_2\text{O}_7^{2-}(aq)\) and measured their absorbances. The calibration curve obtained is represented by the equation:
\[A = 1540 \times C\]
where \(A\) is the absorbance and \(C\) is the concentration of \(\text{Cr}_2\text{O}_7^{2-}(aq)\) in \(\text{mol dm}^{-3}\).
A \(10.0\text{ cm}^3\) sample of the wastewater was diluted to \(250.0\text{ cm}^3\) in a volumetric flask. The absorbance of this diluted solution was measured to be \(0.462\).
(1) Calculate the concentration of \(\text{Cr}_2\text{O}_7^{2-}(aq)\) in the diluted solution. (1 mark)
(2) Calculate the concentration of \(\text{Cr}_2\text{O}_7^{2-}(aq)\) in the original wastewater sample. (2 marks)
(3) State one advantage of using colorimetry over volumetric titration for this analysis. (1 mark)

**Part (c) (5 marks)**
Thin-layer chromatography (TLC) was used to check the purity of a synthesized sample of aspirin (acetylsalicylic acid).
(i) Describe how a TLC plate is prepared and developed to separate the components in the sample. (3 marks)
(ii) Explain how the components can be visualized on the TLC plate, given that aspirin and its impurities are colorless. (1 mark)
(iii) After development, the solvent front traveled \(8.0\text{ cm}\) from the start line. A spot corresponding to aspirin traveled \(3.6\text{ cm}\). Calculate the \(R_f\) value of aspirin. (1 mark)